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dc.contributor.authorSingh, Loushambam H.pt_BR
dc.contributor.authorPati, Sudhanshu Shekharpt_BR
dc.contributor.authorSales, Maria José Araújopt_BR
dc.contributor.authorGuimarães, Edi Mendespt_BR
dc.contributor.authorOliveira, Aderbal Carlos dept_BR
dc.contributor.authorGarg, Vijayendra Kumarpt_BR
dc.date.accessioned2017-12-07T05:12:55Z-
dc.date.available2017-12-07T05:12:55Z-
dc.date.issued2015-11pt_BR
dc.identifier.citationSINGH, Loushambam H. et al. Facile method to tune the particle size and thermal stability of magnetite nanoparticles. Journal of the Brazilian Chemical Society, São Paulo, v. 26, n. 11, p. 2214-2223, nov. 2015. Disponível em: <http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532015001102214&lng=en&nrm=iso>. Acesso em: 16 abr. 2018. doi: http://dx.doi.org/10.5935/0103-5053.20150207.pt_BR
dc.identifier.urihttp://repositorio.unb.br/handle/10482/29692-
dc.language.isoenpt_BR
dc.publisherSociedade Brasileira de Químicapt_BR
dc.rightsAcesso Abertopt_BR
dc.titleFacile method to tune the particle size and thermal stability of magnetite nanoparticlespt_BR
dc.typeArtigopt_BR
dc.subject.keywordMagnetitapt_BR
dc.subject.keywordCrescimentopt_BR
dc.subject.keywordEstabilidadept_BR
dc.rights.licenseJournal of the Brazilian Chemical Society - This is an Open Access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited (CC BY 4.0). Fonte: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532015001102214&lng=en&nrm=iso. Acesso em: 16 abr. 2018.-
dc.identifier.doihttp://dx.doi.org/10.5935/0103-5053.20150207pt_BR
dc.description.abstract1Nucleation and growth mechanism of iron oxide nanoparticles on zeolite template and their stability dependence are reported. Hyperfine field resulting from the variation of particle size indicates the effect of zeolite on particles growth; particle size decreases at lower concentration of zeolite. At higher concentration, a fraction of nano Fe3O4 experiences hyperfine field (45 and 49 T) similar to bulk particles. Effect of incubation and digestion time on the particles growth and the binding effect with zeolite are discussed. Annealing treatments show that the binding of nanoparticles with zeolite stabilizes the nanoparticles with regard to agglomeration and structural transformation. Thermogravimetry-differential thermal analysis (TG-DTA) shows that increase in dehydration temperature from 335.1 to 351.7 K results in zeolite content increasing from 0 to 1000 mg. Weight loss of the particles prepared in incubation time of 0.5 min is 9.46% and reaches 13.9% in 240 min. The weight loss remains practically constant at ca. 9% irrespective of the digestion method.-
dc.description.unidadeInstituto de Física (IF)pt_BR
dc.description.unidadeInstituto de Química (IQ)pt_BR
dc.description.unidadeInstituto de Geociências (IG)pt_BR
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